TīmeklisShare your videos with friends, family, and the world TīmeklisThe synthesis of natural (3R,5R)-1 was initiated from the known epoxide 6, which is commercially available.Treatment of 2-phenylacetaldehyde 7 with 1,3-propanedithiol in the presence of BF 3 ·Et 2 O in CH 2 Cl 2 afforded thioacetal 5 in 90% yield ().The epoxide 6 was coupled with the acyl anion equivalent 5 (1.0 equiv), prepared by …
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